Metals in Air Testing Laboratory

Houston TX metals in air testing laboratory — comprehensive ICP-AES and ICP-MS analysis of 30+ elements simultaneously from a single MCE filter. NIOSH 7300 and 7303 methods. OSHA PEL compliance for lead, arsenic, cadmium, beryllium, chromium, manganese, nickel, and more. ISO/IEC 17025 and AIHA LAP accredited.

ISO/IEC 17025 Accredited AIHA LAP · ID: LAP-101470 Rush Turnaround Available NIOSH 7300 · 7303 · 30+ Metals
Why Metals in Air Testing Matters

Multiple OSHA substance-specific standards with individual action levels — you can't manage what you haven't measured

Multiple OSHA Substance-Specific Standards

Lead, cadmium, beryllium, arsenic, and hexavalent chromium each carry their own OSHA standards with action levels, medical surveillance triggers, and monitoring frequency requirements. A PNOR dust result tells you nothing about these metals — only a full ICP metals scan does.

IARC Group 1 Carcinogens in Workplace Air

Arsenic, cadmium, beryllium, nickel compounds, and hexavalent chromium are all IARC Group 1 confirmed human carcinogens. Occupational exposure to these metals at sub-PEL concentrations over a working career contributes significantly to elevated cancer risk. Targeted ICP analysis is the only way to quantify and reduce that risk.

Unknown Mixtures Require a Full Scan

Abrasive blasting, foundry casting, demolition, and smelting generate airborne particles from materials whose exact metal content may be unknown or variable. A 30+ element ICP scan identifies every metal present simultaneously — you cannot target what you don't know is there. A full ICP metals scan eliminates that blind spot.

Control & Engineering Verification

LEV systems, wet suppression, isolation, and PPE reduce metal concentrations — but only ICP metals monitoring confirms controls maintain exposures below PELs and action levels. Baseline and post-control sampling pairs are the primary documentation for engineering change records and OSHA inspection defense.

ICP Multi-Element Analysis

What Is a Metals in Air Testing Scan?

A metals in air testing scan is the process of collecting airborne particulate on a Mixed Cellulose Ester (MCE) filter using a calibrated personal sampling pump, then dissolving all collected metal particles via acid digestion (nitric/hydrochloric acid) in the laboratory and analyzing the resulting solution by Inductively Coupled Plasma spectrometry.

ICP-AES (Atomic Emission Spectrometry) simultaneously measures the emission spectra of up to 30+ metallic elements from a single digest. ICP-MS (Mass Spectrometry) extends sensitivity to sub-parts-per-billion (ppb) detection for metals with extremely low OSHA action levels — beryllium (0.1 µg/m³), arsenic (5 µg/m³), cadmium (2.5 µg/m³). Both methods are performed in-house at AGT Labs' Houston facility under ISO/IEC 17025 accreditation.

  • 30+ metallic elements detected simultaneously from a single MCE filter digest
  • Results in µg/m³ or mg/m³ compared to OSHA PEL, ACGIH TLV, and NIOSH REL
  • ICP-MS for trace metals requiring sub-ppb detection (Be, As, Cd, Tl, Se)
  • Identifies unknown metal contaminants in complex mixed-metal environments
  • Baseline profiling, periodic compliance monitoring, and control verification sampling
  • OSHA substance-specific standard compliance: Pb, Cd, Be, As, Cr(VI)
Metals in air ICP analysis NIOSH 7300 industrial hygiene air sampling MCE filter OSHA lead cadmium beryllium compliance Houston TX
Full ICP Scan Panel

30+ Metallic Elements Analyzed from One Filter

A single acid digest of one MCE filter provides simultaneous detection of every metal listed below. No separate samples needed — the entire ICP scan panel runs from one collection, one chain-of-custody form, and one analysis.

AGT Labs ICP-AES / ICP-MS Metal Scan Panel — NIOSH 7300 & 7303
30 elements · single acid digest · in-house Houston lab
OSHA Specific Std + IARC Group 1
OSHA Specific Standard
OSHA Z-Table PEL
Full Panel Element
Pb
Lead
82
Cd
Cadmium
48
As
Arsenic
33
Be
Beryllium
4
Ni
Nickel
28
Cr
Chromium
24
Mn
Manganese
25
Fe
Iron
26
Zn
Zinc
30
Cu
Copper
29
Al
Aluminum
13
Co
Cobalt
27
Mo
Molybdenum
42
V
Vanadium
23
Ti
Titanium
22
Sb
Antimony
51
Se
Selenium
34
Ba
Barium
56
Bi
Bismuth
83
Li
Lithium
3
Mg
Magnesium
12
Sn
Tin
50
Sr
Strontium
38
Tl
Thallium
81
W
Tungsten
74
Zr
Zirconium
40
In
Indium
49
Ga
Gallium
31
P
Phosphorus
15
K
Potassium
19

* Panel elements subject to change. Cr(VI) speciation requires separate NIOSH 7605 analysis — total Cr from this ICP scan panel cannot distinguish hexavalent from trivalent chromium. Contact AGT Labs to confirm current panel or request specific element additions.

Regulatory Reference

Key Metals in Air — OSHA PELs, Action Levels & ACGIH TLVs

AGT Labs reports every sample result against OSHA PEL, action level (where applicable), ACGIH TLV, and NIOSH REL. Metals with substance-specific OSHA standards carry additional compliance triggers — medical surveillance, biological monitoring, and enhanced sampling frequency.

MetalOSHA PELOSHA Action LevelACGIH TLVNIOSH RELHealth EffectOSHA StandardRisk
Lead (Pb)50 µg/m³30 µg/m³ — triggers medical surveillance + biological monitoring0.05 mg/m³50 µg/m³CNS, renal, reproductive toxicity; lead poisoning1910.1025IARC 2A
Cadmium (Cd)5 µg/m³2.5 µg/m³ — enhanced monitoring + biological monitoring0.01 mg/m³Lowest feasibleLung cancer, severe renal damage1910.1027IARC Group 1
Inorganic Arsenic (As)10 µg/m³5 µg/m³ — enhanced monitoring + medical surveillance0.01 mg/m³Lowest feasibleLung cancer, skin cancer, peripheral neuropathy1910.1018IARC Group 1
Beryllium (Be)0.2 µg/m³0.1 µg/m³ — extensive program triggers0.00005 mg/m³0.5 µg/m³Chronic beryllium disease (CBD); lung cancer1910.1024IARC Group 1
Hexavalent Chromium Cr(VI)5 µg/m³2.5 µg/m³ — enhanced monitoring + medical surveillance0.01 mg/m³0.2 µg/m³Lung cancer, nasal cancer1910.1026IARC Group 1
Manganese (Mn) Fume1 mg/m³ (ceiling)No formal AL — ACGIH TLV: 0.02 mg/m³0.02 mg/m³1 mg/m³Manganism (irreversible Parkinsonism)Z-Table + 1910.1000Neurotoxin
Nickel (Ni) Compounds1 mg/m³No substance-specific AL0.1 mg/m³0.015 mg/m³Lung and nasal cancer; sensitizationZ-TableIARC Group 1
Cobalt (Co)0.1 mg/m³No substance-specific AL0.02 mg/m³0.05 mg/m³Hard metal lung disease; possible carcinogenZ-TableIARC 2B
Vanadium (V) Dust/Fume0.05 mg/m³ (fume ceiling)No substance-specific AL0.05 mg/m³0.05 mg/m³Respiratory irritation; chemical pneumonitisZ-TableSystemic

* Cr(VI) requires dedicated NIOSH 7605 analysis — total Cr by NIOSH 7300 the ICP scan does not speciate hexavalent vs. trivalent chromium. Beryllium requires ICP-MS (NIOSH 7303) due to sensitivity requirements. Contact AGT Labs for method selection guidance before sampling.

Lab AccreditationISO/IEC 17025:2017
IH Lab AccreditationAIHA LAP · ID: LAP-101470
Environmental TestingPJLA Accredited
Lab LocationHouston TX · In-House ICP
Laboratory Analysis Methods

NIOSH 7300 (ICP-AES) vs. NIOSH 7303 (ICP-MS) — Which Do You Need?

The collection method is identical for both — the difference is what happens in the laboratory. Method selection is driven by which metals are present and what detection sensitivity is required for compliance.

METHOD 01

NIOSH 7300 — ICP-AES

The primary and most widely used ICP method for metals analysis. Acid-digested MCE filter solution is nebulized into an argon plasma at ~6,000–10,000°C, where each element emits light at a characteristic wavelength measured simultaneously by the optical spectrometer. Detects 30+ elements at concentrations typically from 0.01–10,000 µg/m³. Adequate for compliance reporting against most OSHA PELs at standard industrial sampling volumes.

Standard:NIOSH 7300 (ICP-AES)
Detection:~0.01–0.1 µg/filter per element
Best for:Fe, Mn, Pb, Zn, Cu, Ni, Cr, Al — metals at mg/m³ PEL range
Limitation:May not reach LOD for Be, As, Cd at action level concentrations
METHOD 02

NIOSH 7303 — ICP-MS

ICP-MS uses the same plasma ionization as ICP-AES but passes ions through a quadrupole mass spectrometer, separating them by mass-to-charge ratio. This provides detection limits 100–1,000× lower than ICP-AES — reaching 0.0001–0.001 µg/filter. Essential when compliance limits require sub-ppb detection: beryllium (PEL 0.2 µg/m³), inorganic arsenic (PEL 10 µg/m³), cadmium (action level 2.5 µg/m³), and thallium.

Standard:NIOSH 7303 (ICP-MS)
Detection:0.0001–0.001 µg/filter per element (sub-ppb)
Required for:Be, As, Cd, Tl, Se compliance at action level concentrations
Same media:37mm MCE filter, closed-face cassette — identical collection
METHOD 03

NIOSH 7605 — Hexavalent Cr(VI)

Cr(VI) speciation requires a completely separate method and different sampling media from standard ICP collection. NIOSH 7605 (ion chromatography) measures only the hexavalent form of chromium. NIOSH 7300 ICP measures total Cr — it cannot distinguish Cr(VI) from the non-toxic Cr(III). For chromium-generating environments (stainless steel, chrome alloys, chrome plating), always order NIOSH 7605 alongside the standard metals scan. Requires cold-chain shipping (4°C) after collection.

Standard:NIOSH 7605 / OSHA ID-215 (IC)
Media:PVC filter + Na₂CO₃ backup pad — 2-section cassette
Shipping:Refrigerate (4°C), analyze within 14 days
OSHA:PEL 5 µg/m³ · AL 2.5 µg/m³ (1910.1026)
Sampling Decision Guide

When Do You Need a Full Metals in Air Scan?

Not every operation needs a full 30-element panel. Here are the six situations where a full-panel ICP scan — rather than targeted single-metal sampling — is the correct and defensible approach.

01

Unknown Coating, Paint, or Alloy Composition

Abrasive blasting, grinding, cutting, or welding on surfaces where the coating or substrate composition is unknown or variable — structural steel, old industrial equipment, or imported materials with uncertain provenance. The ICP scan identifies the full exposure profile before any control decisions are made.

Use: Full NIOSH 7300 scan + NIOSH 7605 if chromium substrate suspected
02

New Process Baseline Survey

Before establishing a targeted monitoring program for a new manufacturing process, casting operation, or metal processing line — a baseline ICP metals scan establishes which metals are present and at what relative concentrations to drive ongoing program design.

Use: NIOSH 7300 full scan; add NIOSH 7303 if Be, As, or Cd are possible inputs
03

OSHA Inspection Response

Following an OSHA inspection, citation, or hazard complaint — comprehensive ICP metals scan data demonstrates due diligence and provides the quantitative baseline for abatement documentation under any substance-specific standard that applies.

Use: NIOSH 7300 + 7303 for all potentially present metals; rush TAT available
04

Lead Standard Triggering (AL: 30 µg/m³)

Any operation involving lead-painted surfaces (pre-1978 structures), lead-based primers, lead-containing alloys, battery manufacturing, or cable sheathing. The lead action level of 30 µg/m³ triggers medical surveillance and enhanced monitoring under 29 CFR 1910.1025 — ICP compliance monitoring under 29 CFR 1910.1025 is required.

Use: NIOSH 7303 (ICP-MS) for Pb — confirms compliance below AL with certainty
05

Engineering Control Verification

After installation of LEV systems, isolation enclosures, wet suppression, or process substitution — pre/post ICP sampling using the same metals scan panel confirms the magnitude of exposure reduction and documents control effectiveness for OSHA records.

Use: Same NIOSH 7300 panel pre- and post-control to enable direct comparison
06

Foundry, Smelting, or Casting Operations

Metal casting and smelting generate airborne particulate from multiple metals simultaneously — base metal, alloying elements (Mn, Cr, Ni, Mo), and contaminant metals in recycled scrap (Pb, Cd, As). Only a complete ICP metals scan captures the complete occupational exposure picture.

Use: Full NIOSH 7300 + NIOSH 7303 for trace toxic metals (Pb, Cd, As in scrap)
Lab Logistics

Turnaround Times & Sampling Media Supply

Turnaround Options — NIOSH 7300 & 7303
1-Day Rush1 business day+100%
2-Day Rush2 business days+75%
3-Day Rush3 business days+50%
4-Day Rush4 business days+25%
Standard7+ business daysNo Surcharge
Samples received before 2:00 PM CST logged same day. NIOSH 7605 Cr(VI) same TAT schedule — requires cold-chain shipping. Call (713) 453-6090 for rush confirmations.

ICP Metals Sampling Kits

  • 37mm MCE filters (0.8 µm), acid-cleaned, pre-labeled — for NIOSH 7300/7303
  • Closed-face cassette assemblies with end-caps
  • 37mm PVC + Na₂CO₃ backup 2-section cassettes — for Cr(VI) NIOSH 7605 (on request)
  • Calibrated personal air sampling pumps — loaner program
  • Acid-washed tubing and filter holders
  • Field data documentation sheet with metal source / process fields
  • Industrial Hygiene Chain of Custody (COC) form
  • Pre-paid UPS return shipping with cushioned cassette tray
Download IH COC Form

Allow 5 business days for kit dispatch. Houston courier drop-off: (713) 453-6090.

Field Protocol Reference

Metals in Air — Field Sampling Requirements

MCE Filter Setup — NIOSH 7300/7303
Filter setup
37mm MCE filter, 0.8 µm pore, closed-face cassette. Do not use open-face — the closed-face reduces contamination from incidental particle fallout. Do not touch filter surface with bare hands — contamination from skin oils can add metals and affect results.
Do NOT use
PVC filters (used for silica/dust) incompatible with ICP acid digestion — they do not dissolve in acid and interfere with the ICP signal.
Pre-cleaning
Cassettes must be acid-washed. Do not use generic hardware store filter cassettes — contamination will appear as false positive metals.
Field blanks
Minimum 2 field blanks per batch (10% of total samples). Open cassette briefly at the sample location, reseal immediately. Essential for detecting contamination from shipping or handling.
Flow Rates & Sample Volume
Sampling pump
1.7–3.0 L/min. Most personal sampling pumps run at 1.7–2.0 L/min for closed-face cassette collection.
Sample volume
Minimum 200–480 L for a full shift. For trace metal compliance sampling (beryllium, arsenic) near the action level, full-shift sampling is required.
Filter loading
Do not exceed 1 mg total loading for ICP — overloaded filters produce inaccurate results due to incomplete acid digestion.
COC fields
Record: metal sources present (alloy type, coating type), specific processes in operation, LEV status (on/off, hood type), pre- and post-calibration flow, start/stop time, total volume (L), personal or area designation.
Submission Workflow

From Sample Collection to Certified Metals in Air Report

1

Request Media & Pumps

Contact AGT Labs for acid-cleaned MCE kits for this analysis. Specify if Be, As, or Cd monitoring is needed so ICP-MS (NIOSH 7303) is confirmed on your COC alongside NIOSH 7300.

2

Deploy in Breathing Zone

Clip pump to belt; route to lapel. Wear gloves when handling cassettes. Record all metal sources, process, LEV status, and pump calibration flows on COC.

3

Ship to Houston Lab

Seal end-caps. Cr(VI) cassettes: refrigerate (4°C) and ship with ice packs. All samples received before 2:00 PM CST = same-day log-in.

4

Acid Digestion + ICP Analysis

MCE filters undergo HNO₃/HCl acid digestion, then ICP-AES (NIOSH 7300) and/or ICP-MS (NIOSH 7303). 30+ elements quantified from a single digest solution.

5

ICP Metals Compliance Report

Results on secure client portal — µg/m³ per element, OSHA PEL + ACGIH TLV + NIOSH REL comparison, method detection limits, analyst signature, and AIHA LAP accreditation number.

Industries & Clients

Who Relies on AGT Labs for Metals in Air Analysis

Battery Manufacturing & Recycling

Lead-acid battery manufacturing and recycling — highest-volume lead monitoring environment with 29 CFR 1910.1025 action level (30 µg/m³) and blood lead monitoring triggers. NiCd battery work adds cadmium (29 CFR 1910.1027). ICP-MS essential for both at sub-action-level confirmation.

Primary & Secondary Smelting

Primary ore smelting (copper, lead, zinc) and secondary smelting of recycled scrap — complex multi-metal fume mixtures including Pb, As, Cd, and Sb from ore impurities. Full ICP-AES + ICP-MS metals scan panel required to capture the complete profile from scrap feed variability.

Construction Demolition & Abrasive Blasting

Demolition of pre-1978 industrial structures (lead paint), abrasive blasting of steel bridges and tanks (lead and chromium primers), and surface prep on old industrial equipment. The ICP metals scan identifies Pb, Cr, Zn, and other coating-derived metals before respiratory protection selection.

Semiconductor & Electronics Manufacturing

Gallium arsenide (GaAs), indium phosphide (InP), and compound semiconductor manufacturing generate inorganic arsenic and other trace metals requiring ICP analysis at extremely low concentrations. ICP-MS (NIOSH 7303) required for As compliance (PEL 10 µg/m³, action level 5 µg/m³).

IH Consultants & EH&S Programs

Industrial hygiene consulting firms managing multi-client ICP metals scan programs — full ICP panel results with OSHA PEL, ACGIH TLV, and NIOSH REL tri-comparison in every report. Compatible with client EHS platforms. Expert interpretation available on request from AGT Labs staff.

Aerospace & Defense Manufacturing

Beryllium-copper alloy machining, beryllium ceramic manufacturing, titanium grinding, and specialized alloy fabrication all require ICP metals monitoring under the OSHA Beryllium Standard (29 CFR 1910.1024). Beryllium PEL 0.2 µg/m³ demands ICP-MS (NIOSH 7303). Cadmium plating also requires ICP-MS monitoring.

Client Support

Metals in Air Testing — Frequently Asked Questions

What is a metals in air testing scan and when do I need one?
A metals in air testing scan provides comprehensive ICP-AES or ICP-MS analysis that simultaneously identifies and quantifies 30+ metallic elements from a single MCE filter acid digest. You need this ICP scan when: (1) the environment involves multiple metal sources and exact composition is unknown — grinding, blasting, smelting, or demolition; (2) a substance-specific OSHA PEL applies to a metal that may be present — Lead (1910.1025), Cadmium (1910.1027), Beryllium (1910.1024), Arsenic (1910.1018); (3) establishing a baseline for a new industrial process; or (4) verifying engineering control effectiveness post-installation.
What is the OSHA PEL for lead in air?
OSHA's PEL for lead is 50 µg/m³ (8-hour TWA) under 29 CFR 1910.1025 (general industry) and 1926.62 (construction). The action level is 30 µg/m³ — exceeding the AL triggers mandatory enhanced monitoring, medical surveillance, and biological monitoring (blood lead levels). AGT Labs uses ICP-MS (NIOSH 7303) for lead ICP analysis to confirm compliance below the action level with full confidence at very low concentrations.
What is the OSHA PEL for arsenic in air?
OSHA's PEL for inorganic arsenic is 10 µg/m³ (8-hour TWA), with an action level of 5 µg/m³ under 29 CFR 1910.1018. Inorganic arsenic is an IARC Group 1 human carcinogen. ICP-MS (NIOSH 7303) is required for arsenic ICP analysis at these concentrations — ICP-AES detection limits are often inadequate for reliable compliance reporting at the action level. Industries at highest risk include copper smelting, glass manufacturing, semiconductor fabrication, and pesticide/wood preservative production.
What is the OSHA standard for beryllium?
OSHA's new beryllium standard (29 CFR 1910.1024) sets a PEL of 0.2 µg/m³ (8-hour TWA) and an action level of 0.1 µg/m³ — extremely low concentrations that require ICP-MS (NIOSH 7303) for this analysis. Exceeding the action level triggers enhanced monitoring, exposure notification, and a written beryllium control plan. Beryllium-copper alloy machining, aerospace component fabrication, and defense manufacturing are common exposure sources in the Houston industrial base.
How many metals can be analyzed from one air sample?
30 or more metallic elements simultaneously from a single acid digest of one MCE filter — including Al, As, Ba, Be, Cd, Co, Cr, Cu, Fe, Ga, In, K, Li, Mg, Mn, Mo, Ni, P, Pb, Sb, Se, Sn, Sr, Tl, Ti, V, W, Zn, Zr, and Bi. This is the core advantage of ICP metals analysis — a single worker sample provides a complete exposure profile for every potentially hazardous metal in the breathing zone without needing separate filters for each element.
What is the difference between NIOSH 7300 and NIOSH 7303?
Both analyze the same acid digest from the same MCE filter — the difference is the instrument. NIOSH 7300 uses ICP-AES (optical emission) and is suitable for most occupational metals monitoring at mg/m³ OSHA PEL concentrations. NIOSH 7303 uses ICP-MS (mass spectrometry) providing detection limits 100–1,000× lower — essential for Be, As, Cd, and Tl where action levels are in the µg/m³ range and ICP-AES cannot reliably quantify at compliance-relevant concentrations. Both methods use the same MCE cassette — you can request both from a single filter.
Do I need to know which metals are present before metals in air testing?
No — that is the purpose of the metals in air testing scan. A full ICP-AES panel (NIOSH 7300) analyzes all 30+ metals simultaneously regardless of what was suspected. For initial baseline surveys on mixed-metal environments — abrasive blasting, demolition, smelting — a full ICP metals scan is the correct first step. Results then guide targeted ongoing monitoring for specific metals where exposures were identified above action levels.
What are the OSHA PEL and action level for cadmium in air?
OSHA's PEL for cadmium is 5 µg/m³ (8-hour TWA) with an action level of 2.5 µg/m³ under 29 CFR 1910.1027. Cadmium is an IARC Group 1 human carcinogen. ICP-MS (NIOSH 7303) is required for cadmium ICP analysis — ICP-AES detection limits may not achieve the sensitivity needed at the action level concentration. Industries at risk include NiCd battery manufacturing, cadmium electroplating, zinc smelting, brazing with Cd-bearing alloys, and pigment production.
What industries most commonly need metals in air analysis?
Industries requiring routine metals in air testing include: battery manufacturing and recycling (lead, cadmium), primary and secondary smelting (Pb, As, Cd, Ni), abrasive blasting on coated steel (Pb, Cr), foundries and metal casting (multiple metals), mining and ore processing (As, Pb, Cd in ore dust), electronics and semiconductor manufacturing (As, Ga, In, Se), aerospace (Be, Ti, Ni, Cr), soldering operations (Pb, Sn, Ag), plating operations (Cr, Ni, Cd, Zn), and construction demolition of pre-1978 structures (Pb paint).
What turnaround times do you offer for metals in air analysis?
Standard turnaround: 7+ business days at no surcharge. Rush options: 4-day (+25%), 3-day (+50%), 2-day (+75%), 1-day (+100%). Samples received before 2:00 PM CST are logged same day. Call (713) 453-6090 to confirm rush instrument availability for ICP-MS batches.

Ready to Submit Metals in Air Testing Samples?

ISO/IEC 17025 · AIHA LAP · NIOSH 7300 (ICP-AES) · NIOSH 7303 (ICP-MS) · 30+ Elements · Rush TAT · Houston TX

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